Muncy, Geissler, Olds & Lowe, P.C.
Core-shell structure supported tungsten composite catalyst and preparation method and use thereof
The present invention discloses a core-shell structure supported tungsten composite catalyst and a preparation method and use thereof. Most of the existing synthesis methods of the main ring of quinolone drugs have the defects of many synthesis steps, cumbersome operation, large amount of three wastes, higher costs and the like. The present invention prepares a magnetic separable core-shell supported tungsten composite catalyst, WO3/SiO2/Fe3O4, by preparing Fe3O4 colloid and SiO2/Fe3O4 composite nano-particles. This magnetic separable core-shell supported tungsten composite catalyst, WO3/SiO2/Fe3O4, is used to catalyze and synthesize quinolone compounds. The present invention provides an efficient preparation method of quinolone compounds using a catalyst which can be recovered by magnetic separation and recycled. The catalyst prepared by the present invention can be reused in the preparation of quinolone compounds and still retains the original activity without deactivation, which not only greatly improves the production efficiency, but also reduces the environmental pollution.
Hangzhou Normal University Zhejiang Benli Technology Co., Ltd.
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Y02P B01J B01J B01J B01J B01J B01J C07D B01J B01J
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Haining Jun Xiaoling Pengfei Chao
Gu Xu Li Zhang Shen